Salicylaldehyde → HCID 136060540, compound

Participants

Reaction Steps

Prepared as described in the Alkene Formation section using diethyl 4-(6-methylbenzothiazol-2-yl)benzylphosphonate (0.30 g, 0.80 mmol) in dry THF (25 ml), potassium t-butoxide (0.19 g, 1.68 mmol) and 2-hydroxybenzaldehyde (0.097 g, 0.80 mmol) in dry THF (10 ml) to give the title compound (0.16 g, 60%) as a yellow solid after work-up and flash chromatography (1:1 Hexane/EtOAc).

Provenance & Evidence