HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo-1,3-dioxole-5-methylamine → HCID 51301811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo-1,3-dioxole-5-methylamine | HCID 75799 | — |
| Reactant | 5-Isocyanato-1,3-dioxaindane | HCID 5223213 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 51301811 | HCID 51301811 | — |
Reaction Steps
A solution of 3,4-methylenedioxybenzylamine (0.37 g) and 3,4-methylenedioxyphenyl isocyanate (0.4 g) in benzene (25 ml) was refluxed for 1 hour. The precipitate formed was filtered, washed with benzene then dried to give pure DC-0077B (0.78 g, 98%) as a pale brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895554B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-e328678a9dfe414f99e1cc4bfe523da3 |
| Source note | uspto-grants-2014_11 |