HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 339896Generated: October 25, 2026
Tetraethyl orthocarbonate → HCID 68292566, compound
https://huagongshe.com/reaction/339896
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tetraethyl orthocarbonate | HCID 66213 | — |
| Reactant | Biphenyl-4-yl-(3-hydroxyoxetan-3-yl)methanesulfonamide | HCID 68359244 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 68292566 | HCID 68292566 | — |
Reaction Steps
A mixture of 0.17 g of biphenyl-4-yl-(3-hydroxyoxetan-3-yl)methanesulfonamide in 4 ml of tetraethoxymethane and 1 ml of acetic acid was stirred at 90° C. for 3 hours. The solvent was removed under reduced pressure. This gave the crude product, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08895547B2 |
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| Source dataset | uspto-grants-2014_11 |
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| ORD ID | ord-c6b9c90066244e549bc33fd27109c190 |
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| Source note | uspto-grants-2014_11 |
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