HRID339908

反应详情

EQUATION

反应方程式

HRID 339908 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Hydroxy-2-methyl-1-(4-morpholin-4-ylmethylphenyl)propane-1-sulfonamide (350 mg) was stirred with tetramethyl orthocarbonate (5 ml) and glacial acetic acid (1 ml) at 80° C. for 16 hours. The solvents were removed under reduced pressure and the residue was used further without further purification.

WORKUP

后处理

  1. customThe solvents were removed under reduced pressure
  2. customthe residue was used further without further purification