HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 178436933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 178436919 | HCID 178436919 | — |
| Product | HCID 178436933 | HCID 178436933 | 20.6% |
Reaction Steps
The title compound was prepared from (5-chloropyrazin-2-yl)(2-(6-(2-ethyl-5-fluoro-4-hydroxyphenyl)-1H-indazol-3-yl)-6,7-dihydro-1H-imidazo[4,5-c]pyridin-5(4H)-yl)methanone (126 mg, 243 μmol) and cyclohexylamine (48 mg, 487 μmol) using the method of Example 32. The crude material was purified by HPLC Method D to afford (29 mg, 20%) of the title compound as off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895544B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-1d5d3034d0314468b3a2934771d5ad89 |
| Source note | uspto-grants-2014_11 |