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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 340338Generated: October 29, 2026

Dimethylamine → HCID 58213669, compound

https://huagongshe.com/reaction/340338

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
ReactantHCID 86652358HCID 86652358—
ProductHCID 58213669HCID 58213669—

Reaction Steps

4-(2-(5-Amino-8-methylbenzo[f][1,7]naphthyridin-2-yl)ethyl)-N,N,3-trimethylbenzamide was prepared from 4-(2-(5-amino-8-methylbenzo[f][1,7]naphthyridin-2-yl)ethyl)-3-methylbenzoyl chloride (Example 116/Step 2) and dimethylamine following the procedures described for Example 117. 1H NMR (CDCl3): δ 8.68 (s, 1H), 8.32 (s, 1H), 8.04 (d, 1H), 7.66 (s, 1H), 7.31 (d, 1H), 7.06-7.18 (m, 3H), 3.08-3.19 (m, 4H), 2.96 (d, 3H), 2.54 (s, 3H), 2.33 (s, 3H), 2.05 (s, 3H). LRMS [M+H]=399.2

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08895577B2
Source datasetuspto-grants-2014_11
ORD IDord-4b7797a21ce145c4b4e15d88d42c29c1
Source noteuspto-grants-2014_11