HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 58213669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 86652358 | HCID 86652358 | — |
| Product | HCID 58213669 | HCID 58213669 | — |
Reaction Steps
4-(2-(5-Amino-8-methylbenzo[f][1,7]naphthyridin-2-yl)ethyl)-N,N,3-trimethylbenzamide was prepared from 4-(2-(5-amino-8-methylbenzo[f][1,7]naphthyridin-2-yl)ethyl)-3-methylbenzoyl chloride (Example 116/Step 2) and dimethylamine following the procedures described for Example 117. 1H NMR (CDCl3): δ 8.68 (s, 1H), 8.32 (s, 1H), 8.04 (d, 1H), 7.66 (s, 1H), 7.31 (d, 1H), 7.06-7.18 (m, 3H), 3.08-3.19 (m, 4H), 2.96 (d, 3H), 2.54 (s, 3H), 2.33 (s, 3H), 2.05 (s, 3H). LRMS [M+H]=399.2
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895577B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-4b7797a21ce145c4b4e15d88d42c29c1 |
| Source note | uspto-grants-2014_11 |