HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl (2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate → 2-(Mesitylethynyl)benzo[f][1,7]naphthyridin-5-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl (2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate | HCID 2773231 | — |
| Reactant | 3-Chloro-5-(mesitylethynyl)picolinonitrile | HCID 66874949 | — |
| Product | 2-(Mesitylethynyl)benzo[f][1,7]naphthyridin-5-amine | HCID 66893310 | — |
Reaction Steps
2-(Mesitylethynyl)benzo[f][1,7]naphthyridin-5-amine was prepared from 3-chloro-5-(mesitylethynyl)picolinonitrile (Example 77/Step 1) and tert-butyl 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarbamate (commercially available) following the procedures described for Example 45/Step 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895577B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-423534b1a41e46f9a91db2b334aabe28 |
| Source note | uspto-grants-2014_11 |