HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68028001, compound → 1354223-61-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68028001 | HCID 68028001 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1354223-61-2 | HCID 84062139 | 109.4% |
Reaction Steps
A methanol (20 ml) solution containing 1-(5-nitropyridin-2-yl)pyrrolidin-2-one (31 mg) was prepared and subjected to a hydrogenation reaction (30° C.; 1 bar; flow rate: 1 ml/min; 10% Pd/C) using H-cube™. Then, the solvent was distilled away under reduced pressure, and a purple solid of 1-(5-aminopyridin-2-yl)pyrrolidin-2-one (29 mg) was thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895585B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-c0527acb91e64c37af7bcc074c8b38d3 |
| Source note | uspto-grants-2014_11 |