N-Iodosuccinimide → HCID 178506569, compound

HRID 34060Notes

Reaction equation

[I:1]N1C(=O)CCC1=O.[NH:9]1[C:17]2[C:12](=[N:13][CH:14]=[CH:15][CH:16]=2)[CH:11]=[N:10]1>>[I:1][C:11]1[C:12]2=[N:13][CH:14]=[CH:15][CH:16]=[C:17]2[NH:9][N:10]=1

Participants

Reactant 2

HCID 120273N-Iodosuccinimide

HCID 216436531H-Pyrazolo(4,3-b)pyridine

Product 1

HCID 178506569HCID 178506569, compoundYield 57.4%

Procedure

In the similar method as described in Production example 206, 9.5 g of N-iodosuccinimide was reacted on 5 g of 1H-pyrazolo[4,3-b]pyridine, to afford 5.9 g of the title compound as a colorless powder.

Sources & evidence

ORD record: ord-50872ac1949e49fc8cd3aadf0d9dce2d
Source dataset: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07429609B2

Reaction notes

Loading…