HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58282163, compound → HCID 58282131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58282163 | HCID 58282163 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Diisopropylamine | HCID 7912 | — |
| Product | HCID 58282131 | HCID 58282131 | — |
Reaction Steps
The cleavable diol is made in the following manner. To a solution of compound (73) in methylene chloride, diisopropylamine is added and the solution is stirred until reaction is complete. A standard aqueous workup is done and the diol should remain in the organic phase. Evaporate the solvent and collect bis(4-hydroxy-2-methylbutan-2-yl)oxalate (74).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895691B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-b98b9e1f6c8e4f7cb5aa178d9a07551c |
| Source note | uspto-grants-2014_11 |