HCID 58319893, compound → HCID 58319897, compound

Participants

Reaction Steps

The crude product (106) was combined with aqueous sodium bicarbonate solution (20 mL, 0.75 N) and stirred for 3 days. The compound was then extracted using ethyl acetate in three 20 mL portions. The organic phase was then evaporated and separated in a column to get a clear oil.) 1H NMR (CDCl3): δ 1.19 (s, 3H), 1.43 (s, 3H), 1.61 (s, 3H), 1.75 (t, 2H), 2.00 (m, 1H), 2.36 (t, 2H), 2.63 (s, 2H), 3.98 (s, 2H), 4.16 (s, 2H), 5.27 (s, 1H), 5.68 (s, 1H).

Provenance & Evidence