HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → 1-Boc-1-methylhydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Di-tert-butyl dicarbonate | HCID 90495 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Boc-1-methylhydrazine | HCID 3748280 | — |
Reaction Steps
10 mL of methyl hydrazine was dissolved in 90 mL of ethanol, and under stirring at ice-cooling, a solution of 41 g of di-tert-butyldicarbonate in 90 mL of ethanol was added dropwise over 45 minutes. After stirring at room temperature for 7 hours, the solvent was evaporated, to afford 24.7 g of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07429609B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-fc6875eeb4de43a8bab93f777795ac96 |
| Source note | uspto-grants-2008_09 |