Ethyl isocyanate → HCID 59320942, compound

Participants

Reaction Conditions

Reaction Steps

To 2-amino-4-chloropyridine (1.02 g, 7.9 mmol) in THF (20 mL) was added ethyl isocyanate (0.69 ml, 8.69 mmol) and the reaction heated at 55° C. for 18 hours. The reaction was concentrated in vacuo. The resulting white solid was suspended in EtOAc and filtered to give the product as a white solid (0.79 g).

Provenance & Evidence