HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(Chlorocarbonyl)phenyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Acetoxybenzoic acid | HCID 238669 | — |
| Product | 3-(Chlorocarbonyl)phenyl acetate | HCID 12998558 | 99% |
Reaction Steps
Using the above procedure, reaction of with thionyl chloride (11.1 mL, 15.3 mmol) and 3-acetoxybenzoic acid (2.50 g, 13.9 mmol) gave 511 (2.72 g, 99%) as a colorless oil. This material was used in the next step without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895752B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-0532de99dffc4e219aa9a7c1fb11c578 |
| Source note | uspto-grants-2014_11 |