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HRID341555

反应详情

EQUATION

反应方程式

HRID 341555 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N1CC[C@H](O)C1
HCID854055

tert-Butyl (3S)-3-hydroxypyrrolidine-1-carboxylate

C9H17NO3

结构：CC(C)(C)OC(=O)N1CC[C@H](Oc2ccccc2)C1
HCID69333485

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CC[C@@H](Oc2ccccc2)C1
HCID86610018

未命名化合物

收率 51%

PROCEDURE

实验过程

tert-Butyl (3R)-3-phenoxypyrrolidine-1-carboxylate was prepared from tert-butyl (3S)-3-hydroxypyrrolidine-1-carboxylate (0.43 g, 2.286 mmol) according to the method described for Intermediate 270 to afford the title compound (0.312 g, 51% yield). Method B HPLC-MS: MH+ requires m/z=208 Found: m/z=208, Rt=2.20 min (100%).