Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Permanganate | HCID 516875 | — |
| Reactant | HCID 54238168 | HCID 54238168 | — |
| Product | HCID 54412755 | HCID 54412755 | — |
Reaction Steps
Potassium permanganate (33.66 g) was added in portions to a stirred heated suspension of 2,4-dichloro-3-(methylsulphonyl)toluene (16.88 g) in water at 95°-100° C. The mixture was stirred and heated at reflux for one and a half hours. The hot suspension was filtered and the filtrate was cooled to 0° C. and acidified. It was filtered to give 2,4-dichloro-3-(methylsulphonyl)benzoic acid (5.35 g) as an orange solid, m.p. 157.5°-158.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05856274 |
|---|
| Source dataset | uspto-grants-1999_01 |
|---|
| ORD ID | ord-2b0982a8fc1c416f89bdded43c1e0f12 |
|---|
| Source note | uspto-grants-1999_01 |
|---|
