HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 341980Generated: October 30, 2026
Diethyl Ether → Ethyl 3-(acetylsulfanyl)-2-methylpropanoate
https://huagongshe.com/reaction/341980
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Ethyl Methacrylate | HCID 7343 | — |
| Reactant | 2-Thiopheneacetic acid | HCID 15970 | — |
| Product | Ethyl 3-(acetylsulfanyl)-2-methylpropanoate | HCID 15289598 | — |
Reaction Steps
Ethyl 2-methylpropenoate (39 mmol) was diluted with 5.6 mL (78 mmol) of thiolacetic acid and stirred at 65° C. for 36 h. The mixture was then diluted with ether, washed with water and the organic phase was dried with Na2SO4. Evaporation to dryness yielded the title material as an orange oil which was used as such for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05856322 |
|---|
| Source dataset | uspto-grants-1999_01 |
|---|
| ORD ID | ord-67c4aba80bb94ed1b303e73ecebdaacc |
|---|
| Source note | uspto-grants-1999_01 |
|---|
