Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Methylallylamine → (E)-allyl-[4-[4-(6-bromo-benzo[d]isoxazol-3-yl)-phenoxy]-but-2-enyl]-methyl-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Methylallylamine | HCID 69391 | — |
| 반응물 | trans-1,4-Dibromo-2-butene | HCID 641245 | — |
| 반응물 | (E)-6-bromo-3-[4-(4-bromo-but-2-enyloxy)-phenyl]-benzo[d]isoxazole | HCID 67596916 | — |
| 반응물 | 4-(6-Bromo-benzo[d]isoxazol-3-yl)-phenol | HCID 136365325 | — |
| 생성물 | (E)-allyl-[4-[4-(6-bromo-benzo[d]isoxazol-3-yl)-phenoxy]-but-2-enyl]-methyl-amine | HCID 67598617 | — |
반응 단계
Analogously to Example 14d, from 4-(6-bromo-benzo[d]isoxazol-3-yl)-phenol and (E)-1,4-dibromo-2-butene via (E)-6-bromo-3-[4-(4-bromo-but-2-enyloxy)-phenyl]-benzo[d]isoxazole and by reaction with N-allyl-methyl-amine there is obtained (E)-allyl-[4-[4-(6-bromo-benzo[d]isoxazol-3-yl)-phenoxy]-but-2-enyl]-methyl-amine which is converted into the fumarate, MS: m/e 413 (M+H+, 1 Br).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05856503 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-5875efb8520d4946bac61c8e38102eda |
| 출처 메모 | uspto-grants-1999_01 |