m-Chloroperbenzoic acid → HCID 178512310, compound

Participants

Reaction Steps

From the compound of Example 11 (340 mg, 0.62 mmol) and 50% m-chloroperbenzoic acid as a white solid (200 mg). 1Hnmr (300 MHz, CDCl3) δ 3.27 (2H, d, J 8.0 Hz), 4.14 (1H, t, J 7.86 Hz), 4.48 (2H, d, J 5.72 Hz), 5.29 (1H, br), 6.48 (2H, t, J 73.49 Hz), 6.85 (2H, d, J 7.02 Hz), 7.00 (1H, dd, J 2.19, 8.43 Hz), 7.06 (1H, br), 7.12-7.34 (1OH, c), 7.50 (1H, br) and 7.98 (2H, d, J 7.03 Hz). m/z (ESI, 60V) 580 (MH+, 85), 538 (100), 429 (41).

Provenance & Evidence