Carbon Disulfide → HCID 10979641, compound

Participants

Reaction Steps

5.7 g of carbon disulphide and 22 ml of triethylamine are mixed in keeping a temperature below 10° C. by an ice-bath. 10 g of 3-chloroaniline dissolved in 10 ml of absolute ethanol are added and the reaction mixture is stirred and left to return to ambient temperature. After 24 h, the yellow precipitate obtained is filtered off, washed with ethanol then with pentane.

Provenance & Evidence