HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54263157, compound → HCID 53692562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54263157 | HCID 54263157 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53692562 | HCID 53692562 | — |
Reaction Steps
7-Butyroyloxy-3-ethyl-8-(2-propenyl)coumarin (Step B; 95 mg) dissolved in methanol was reacted with 10% Pd/C under an atmosphere of hydrogen gas for several hours. The crude mixture was loaded directly onto a flash column containing silica gel and eluted with 20% ethyl acetate/hexane. This provided the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05859051 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-b853e57eeb8742969212c496c26aaf9c |
| Source note | uspto-grants-1999_01 |