Boron tribromide → HCID 178480851, compound

HRID 34278Notes

Reaction equation

HRID 34278 reaction equation
B(Br)(Br)Br.[SH:5][C:6]1[N:10]([CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([O:18]C)[CH:13]=2)[C:9]([CH2:20][N:21]2[CH2:26][CH2:25][N:24]([CH3:27])[CH2:23][CH2:22]2)=[N:8][N:7]=1>C(Cl)Cl>[SH:5][C:6]1[N:10]([CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([OH:18])[CH:13]=2)[C:9]([CH2:20][N:21]2[CH2:22][CH2:23][N:24]([CH3:27])[CH2:25][CH2:26]2)=[N:8][N:7]=1

Participants

4

Reactant 2

HCID 25134Boron tribromideHCID 178490271HCID 178490271, compound

Product 1

HCID 178480851HCID 178480851, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Reaction according to standard procedures of boron tribromide (40% BBr3 in methylene chloride) with 3-mercapto-4-(3-methoxybenzyl)-5-[(4-methyl-1-piperazinyl)methyl]-1,2,4-triazole in methylene chloride yields 3-mercapto-4-(3-hydroxybenzyl)-5-[(4-methyl-1-piperazinyl)methyl]-1,2,4-triazole.

Workup

  1. customReaction

Sources & evidence

ORD record
ord-6cb9a50e5e664c3bba95b1d803799f50
Source dataset
uspto-grants-1988_08
Patent number
US04761415

Reaction notes

Loading…