4-Hydroxybenzoic Acid → HCID 67570688, compound

Participants

Reaction Conditions

Reaction Steps

1500 g of methyl isobutyl ketone, 69 g of 4-hydroxybenzoic acid and 58.0 g of triethylamine were charged into a separable flask as used in Reference Example 4, and after the flask was heated to 80° C. while replacing the flask inside atmosphere with a nitrogen gas, 72.4 g of p-chloromethylstyrene was dropwise added thereto over 2 hours. Then, stirring was continued for 6 hours. After the reaction, 3 liters water was added to the reaction mixture, and powdery precipitate was recovered therefrom and washed with n-hexane, whereby 36.2 g of p-hydroxybenzoyloxymethylstyrene of the following chemical formula was obtained (yield: 30%): ##STR8##

Provenance & Evidence