HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3'-(Trimethylenedioxy)di-p-anisaldehyde → HCID 178491251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3'-(Trimethylenedioxy)di-p-anisaldehyde | HCID 21195017 | — |
| Reactant | HCID 178418668 | HCID 178418668 | — |
| Catalyst | HCID 178478830 | HCID 178478830 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178491251 | HCID 178491251 | 86.5% |
Reaction Steps
3,3'-(trimethylenedioxy)di-p-anisaldehyde (1.032 g), aminoguanidine hydrochloride (0.829 g), and aminoguanidine dihydrochloride (0.02 g) were heated in 95% methanol (10.5 mL) for 16 hr. Cooling and filtration gave 1.372 g of 3,3'-(trimethylenedioxy)di-p-anisaldehyde bis(amidinohydrazone)dihydrochloride, mp 233°-5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05859062 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-229aa35f3eab4e1b9b210bd215dc702d |
| Source note | uspto-grants-1999_01 |