HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triisopropyl borate → Boronic acid, [3-fluoro-4-(octyloxy)phenyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triisopropyl borate | HCID 21531 | — |
| Reactant | Benzene, 4-bromo-2-fluoro-1-(octyloxy)- | HCID 3581959 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | Boronic acid, [3-fluoro-4-(octyloxy)phenyl]- | HCID 10611926 | — |
Reaction Steps
This was prepared using a similar method to that described for compound 5. Quantities: 1-bromo-3-fluoro-4-octoxybenzene (15 g, 0.05 mol), n-butyllithium (5 ml, 10M in hexane, 0.05 mol), tri-isopropylborate (18.81 g, 0.1 mol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05861109 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-aa9188e7d9fa41eb84aa59de167ab655 |
| Source note | uspto-grants-1999_01 |