HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Methyl 2-[5-chloro-2-[4-(4-chloro-5-difluoromethoxy-1-methylpyrazol-3-yl)phenylthiomethyl]phenoxy]propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 2-(2-chloromethyl-5-chlorophenoxy)propionate | HCID 53768369 | — |
| Reactant | 4-(4-Chloro-5-difluoromethoxy-1-methylpyrazol-3-yl)thiophenol | HCID 135960884 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 2-[5-chloro-2-[4-(4-chloro-5-difluoromethoxy-1-methylpyrazol-3-yl)phenylthiomethyl]phenoxy]propanoate | HCID 67703361 | — |
Reaction Steps
This compound is prepared in a manner analogous to that of Step I of Example 1, using 0.58 gram (0.002 mole) of 4-(4-chloro-5-difluoromethoxy-1-methylpyrazol-3-yl)thiophenol, 0.32 gram (0.002 mole) of methyl 2-(5-chloro-2-chloromethylphenoxy)propanoate (prepared as in Steps A through D of Example 2), and 0.41 gram (0.003 mole) of potassium carbonate in 60 mil of N,N-di-methylformamide, yielding the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05861359 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-9a7c099280614c60a3dab91b2277e432 |
| Source note | uspto-grants-1999_01 |