Boron tribromide → HCID 53722094, compound

HRID 343292Notes

Reaction equation

HRID 343292 reaction equation
[Cl:1][C:2]1[N:6]([CH:7]([CH3:9])[CH3:8])[C:5]([CH3:10])=[N:4][C:3]=1[C:11]1[CH:16]=[CH:15][C:14]([O:17]C)=[CH:13][CH:12]=1.B(Br)(Br)Br>C(Cl)Cl>[Cl:1][C:2]1[N:6]([CH:7]([CH3:9])[CH3:8])[C:5]([CH3:10])=[N:4][C:3]=1[C:11]1[CH:12]=[CH:13][C:14]([OH:17])=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 25134Boron tribromideHCID 54388388HCID 54388388, compound

Product 1

HCID 53722094HCID 53722094, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

This compound is prepared in a manner analogous to that of Step H of Example 1, using 2.6 grams (0.010 mole) of 5-chloro-1-(1-methylethyl)-4-(4-methoxyphenyl)-2-methylimidazole and 20 mL (0.020 mole) of 1M boron tribromide (in methylene chloride) in 50 mL of methylene chloride, yielding 4-[5-chloro-1-(1-methylethyl)-2-methylimidazol-4-yl]phenol.

Workup

  1. customThis compound is prepared in a manner analogous to that of Step H of Example 1

Sources & evidence

ORD record
ord-755042d4a9fb40bbb04d667a170bb5d7
Source dataset
uspto-grants-1999_01
Patent number
US05861359

Reaction notes

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