HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 178525732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Formic acid, copper salt | HCID 44152240 | — |
| Reactant | HCID 178525731 | HCID 178525731 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178525732 | HCID 178525732 | 40.5% |
Reaction Steps
2.58 g of 1,4-trans-cyclohexane dicarboxylic acid was dissolved under heating in a mixture solvent of 100 cm3 of methanol and 20 cm3 of formic acid. After this solution was cooled to the normal temperature, into this solution under stirring, a further solution in which 3.38 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 1.43 g of 1,4-trans-cyclohexane dicarboxylic acid copper was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05862796 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-c01f4852e5434038b46b74957eb732e9 |
| Source note | uspto-grants-1999_01 |