HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorine → HCID 53829400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | 2-Nitro-4-(trifluoromethanesulfonyl)aniline | HCID 4529469 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 53829400 | HCID 53829400 | 95.3% |
Reaction Steps
Analogously to Example 14, 27 g of 2-nitro-4-trifluoromethylsulphonyl-aniline in 100 ml of acetic acid were chlorinated with 10 g of chlorine. 29 g of 2-nitro-4-trifluoromethylsulphonyl-6-chloro-aniline were obtained, melting point: 138°-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05863933 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-de63a659b589408eb10d5cccc9a53069 |
| Source note | uspto-grants-1999_01 |