HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 21846250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 21846221 | HCID 21846221 | — |
| Product | HCID 21846250 | HCID 21846250 | — |
Reaction Steps
Compounds of Formula I are alternatively prepared by the treatment of 4-(4-fluoronaphth-1-yl)-6-isopropyl-2-methanesulfonylpyrimidine with aniline in the absence of solvent at a higher temperatures of 120° C. to afford 4-(4-fluoronaphth-1-yl)-6-isopropyl-2-phenylaminopyrimidine, m.p. 85.7°-86.3° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05863924 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-b25b456288054815bfcf7178e6d96e4b |
| Source note | uspto-grants-1999_01 |