HCID 86753631, compound → HCID 86753630, compound

HRID 344068Notes

Reaction equation

HRID 344068 reaction equation
[CH3:1][N:2](C)[C:3]1[CH:4]=[CH:5][C:6]([N+:36]([O-:38])=[O:37])=[C:7]([N:9]([CH2:16][C:17]2[CH:22]=[CH:21][C:20]([C:23]3[C:24]([C:29]([O:31][C:32]([CH3:35])([CH3:34])[CH3:33])=[O:30])=[CH:25][CH:26]=[CH:27][CH:28]=3)=[CH:19][CH:18]=2)[C:10](=[O:15])[CH2:11][CH2:12][CH2:13][CH3:14])[CH:8]=1>CCCCCC.C(OCC)(=O)C>[CH2:1]([NH:2][C:3]1[CH:4]=[CH:5][C:6]([N+:36]([O-:38])=[O:37])=[C:7]([N:9]([CH2:16][C:17]2[CH:18]=[CH:19][C:20]([C:23]3[C:24]([C:29]([O:31][C:32]([CH3:35])([CH3:33])[CH3:34])=[O:30])=[CH:25][CH:26]=[CH:27][CH:28]=3)=[CH:21][CH:22]=2)[C:10](=[O:15])[CH2:11][CH2:12][CH2:13][CH3:14])[CH:8]=1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

3

Reactant 1

HCID 86753631HCID 86753631, compound

Product 1

HCID 86753630HCID 86753630, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

tert.butyl 4'-[N-(5-dimethylamino-2-nitrophenyl)-pentanoylaminomethyl]biphenyl-2-carboxylate oil, Rf value: 0.35 (Silica gel: hexane/ethyl acetate=4:1).

Sources & evidence

ORD record
ord-8e520f266d4341f4ad6fe2b14d554adb
Source dataset
uspto-grants-1999_01
Patent number
US05864043

Reaction notes

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