HCID 15069167, compound → HCID 15069153, compound

HRID 344070Notes

Reaction equation

HRID 344070 reaction equation
C(O[C:6]1[C:11]2[N:12]([CH2:19][C:20]3[CH:25]=[CH:24][C:23]([C:26]4[C:27]([C:32]([O:34][C:35]([CH3:38])([CH3:37])[CH3:36])=[O:33])=[CH:28][CH:29]=[CH:30][CH:31]=4)=[CH:22][CH:21]=3)[C:13]([CH2:15][CH2:16]CC)=[N:14][C:10]=2[C:9](C)=[CH:8][CH:7]=1)CCC>C(Cl)Cl.C(O)C>[CH2:15]([C:13]1[N:12]([CH2:19][C:20]2[CH:21]=[CH:22][C:23]([C:26]3[C:27]([C:32]([O:34][C:35]([CH3:38])([CH3:36])[CH3:37])=[O:33])=[CH:28][CH:29]=[CH:30][CH:31]=3)=[CH:24][CH:25]=2)[C:11]2[CH:6]=[CH:7][CH:8]=[CH:9][C:10]=2[N:14]=1)[CH3:16]

Participants

3

Reactant 1

HCID 15069167HCID 15069167, compound

Product 1

HCID 15069153HCID 15069153, compound

Reagents, catalysts & solvents 1

HCID 21584144Dichloromethane ethanolSolvent

Procedure

tert.butyl 4'-[(7-n-butoxy-2-n-butyl-4-methyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate oil, Rf value: 0.55 (Silica gel: methylene chloride/ethanol=19:1)

Sources & evidence

ORD record
ord-56a721bec9f84cb8b242de72d76fdd62
Source dataset
uspto-grants-1999_01
Patent number
US05864043

Reaction notes

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