HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert.-butyl 4'-[(2-n-butyl-6-carboxy-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate → Tert.butyl 4'-[(2-(4-hydroxyphenyl)-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert.-butyl 4'-[(2-n-butyl-6-carboxy-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate | HCID 15069195 | — |
| Reactant | DCM MeOH AcOH | HCID 21877243 | — |
| Product | Tert.butyl 4'-[(2-(4-hydroxyphenyl)-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate | HCID 136333559 | — |
Reaction Steps
tert.butyl 4'-[(2-n-butyl-6-carboxy-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate oil, Rf value: 0.90 (Silica gel: methylene chloride/methanol/acetic acid=9:0.8:0.2)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05864043 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-95c3bea38fb54a98b2ad9d1bbbaf464a |
| Source note | uspto-grants-1999_01 |