HCID 67572630, compound → HCID 15104336, compound

HRID 344076Notes

Reaction equation

HRID 344076 reaction equation
[CH2:1]([NH:4][C:5]([NH:7][C:8]1[CH:9]=[CH:10][C:11]2[N:15]=[C:14]([CH2:16][CH2:17][CH2:18][CH3:19])[N:13]([CH2:20][C:21]3[CH:26]=[CH:25][C:24]([C:27]4[C:28]([C:33]([O:35][C:36]([CH3:39])([CH3:38])[CH3:37])=[O:34])=[CH:29][CH:30]=[CH:31][CH:32]=4)=[CH:23][CH:22]=3)[C:12]=2[CH:40]=1)=[O:6])[CH:2]=[CH2:3]>C(Cl)Cl.C(O)C>[CH2:16]([C:14]1[N:13]([CH2:20][C:21]2[CH:22]=[CH:23][C:24]([C:27]3[C:28]([C:33]([O:35][C:36]([CH3:39])([CH3:38])[CH3:37])=[O:34])=[CH:29][CH:30]=[CH:31][CH:32]=3)=[CH:25][CH:26]=2)[C:12]2[CH:40]=[C:8]([NH:7][C:5]([NH:4][CH2:1][C:2]3[CH:12]=[CH:40][CH:8]=[CH:9][CH:3]=3)=[O:6])[CH:9]=[CH:10][C:11]=2[N:15]=1)[CH2:17][CH2:18][CH3:19]

Participants

3

Reactant 1

HCID 67572630HCID 67572630, compound

Product 1

HCID 15104336HCID 15104336, compound

Reagents, catalysts & solvents 1

HCID 21584144Dichloromethane ethanolSolvent

Procedure

tert.butyl 4'-[(6-allylaminocarbonylamino-2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate oil, Rf value: 0.10 (Silica gel: methylene chloride/ethanol=19:1)

Sources & evidence

ORD record
ord-1311ed07fc994825be3c3a3b2d64705a
Source dataset
uspto-grants-1999_01
Patent number
US05864043

Reaction notes

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