HCID 15069238, compound → HCID 15069235, compound

HRID 344079Notes

Reaction equation

[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[C:18]([C:23]([O:25][C:26]([CH3:29])([CH3:28])[CH3:27])=[O:24])=[CH:19][CH:20]=[CH:21][CH:22]=3)=[CH:13][CH:12]=2)[C:8]2[CH:30]=[C:31]([NH:34][C:35]([O:37]CC)=O)[CH:32]=[CH:33][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4].[CH2:40](Cl)Cl.[CH2:43](O)[CH3:44]>>[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:12]=[CH:13][C:14]([C:17]3[C:18]([C:23]([O:25][C:26]([CH3:29])([CH3:27])[CH3:28])=[O:24])=[CH:19][CH:20]=[CH:21][CH:22]=3)=[CH:15][CH:16]=2)[C:8]2[CH:7]=[CH:33][CH:32]=[C:31]([NH:34][C:35](=[O:37])[CH2:40][CH2:43][CH3:44])[C:30]=2[N:6]=1)[CH2:2][CH2:3][CH3:4]

Participants

Reactant 2

HCID 15069238HCID 15069238, compound

HCID 21584144Dichloromethane ethanol

Product 1

HCID 15069235HCID 15069235, compound

Procedure

tert.butyl 4'-[(2-n-butyl-6-ethoxycarbonylamino-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate amorphous substance, Rf value: 0.30 (Silica gel: methylene chloride/ethanol=19:1)

Sources & evidence

ORD record: ord-7570d5e1e6494410bd02b89a97249260
Source dataset: uspto-grants-1999_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05864043

Reaction notes

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