HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57134023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86749685 | HCID 86749685 | — |
| Product | HCID 57134023 | HCID 57134023 | 85.7% |
Reaction Steps
Prepared in analogous manner to Example 9 from tert.butyl 4'-[(2-n-butyl-6-(N-methylaminocarbonyl-methylamino)-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate and trifluoroacetic acid. Yield: 85.7% of theoretical, Melting point: 163°-165° C. C29H30N4O3 (470.58) Calculated: C 71.46, H 6.42, N 11.91 Found: 71.33, 6.64, 11.74
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05864043 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-ce6bc5b3caae48acba21d6e75294bd87 |
| Source note | uspto-grants-1999_01 |