Sodium azide ammonium chloride → HCID 178441507, compound

HRID 344217Notes

Reaction equation

HRID 344217 reaction equation
[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][C:18]=3[C:24]#[N:25])=[CH:13][CH:12]=2)[C:8]2[CH:26]=[C:27]([N:30]([CH3:40])[C:31]([NH:33][CH:34]3[CH2:39][CH2:38][CH2:37][CH2:36][CH2:35]3)=[O:32])[CH:28]=[CH:29][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4].[Cl-].[NH4+].[N-:43]=[N+:44]=[N-:45].[Na+]>>[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][C:18]=3[C:24]3[NH:45][N:44]=[N:43][N:25]=3)=[CH:13][CH:12]=2)[C:8]2[CH:26]=[C:27]([N:30]([CH3:40])[C:31]([NH:33][CH:34]3[CH2:35][CH2:36][CH2:37][CH2:38][CH2:39]3)=[O:32])[CH:28]=[CH:29][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 21923157Sodium azide ammonium chlorideHCID 572513924'-[(2-n-butyl-6-(N-cyclohexylaminocarbonyl-methyl-amino)-benzimidazol-1-yl)-methyl]-4-chloro-2-cyano-biphenyl

Product 1

HCID 178441507HCID 178441507, compound

Procedure

Prepared in analogous manner to Example 59 from 4'-[(2-n-butyl-6-(N-cyclohexylaminocarbonyl-methyl-amino)-benzimidazol-1-yl)-methyl]-4-chloro-2-cyano-biphenyl and ammonium chloride/sodium azide.

Sources & evidence

ORD record
ord-1adbceda3b6d4384b5a0be199b796420
Source dataset
uspto-grants-1999_01
Patent number
US05864043

Reaction notes

Loading…