Sodium azide ammonium chloride → HCID 178441510, compound

HRID 344225Notes

Reaction equation

HRID 344225 reaction equation
C([N:5]1[C:9]2[CH:10]=[CH:11][C:12]([NH:14][C:15]([NH:17][CH:18]3[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]3)=[O:16])=[CH:13][C:8]=2[N:7]([CH2:24][C:25]2[CH:30]=[CH:29][C:28]([C:31]3[CH:36]=[C:35]([Cl:37])[CH:34]=[CH:33][C:32]=3[C:38]#[N:39])=[CH:27][CH:26]=2)[CH2:6]1)CCC.[N-:40]=[N+:41]=[N-:42].[Na+].[Cl-].[NH4+]>>[CH2:13]([C:6]1[N:7]([CH2:24][C:25]2[CH:26]=[CH:27][C:28]([C:31]3[CH:36]=[C:35]([Cl:37])[CH:34]=[CH:33][C:32]=3[C:38]3[NH:39][N:42]=[N:41][N:40]=3)=[CH:29][CH:30]=2)[C:8]2[CH:13]=[C:12]([NH:14][C:15]([NH:17][CH:18]3[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]3)=[O:16])[CH:11]=[CH:10][C:9]=2[N:5]=1)[CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 21923157Sodium azide ammonium chlorideHCID 675730544'-[(3-n-butyl-6-(N-cyclohexylaminocarbonylamino)-benzimidazol-1-yl)-methyl]-5-chloro-2-cyano-biphenyl

Product 1

HCID 178441510HCID 178441510, compound

Procedure

Prepared in analogous manner to Example 59 from 4'-[(3-n-butyl-6-(N-cyclohexylaminocarbonylamino)-benzimidazol-1-yl)-methyl]-5-chloro-2-cyano-biphenyl and sodium azide/ammonium chloride.

Sources & evidence

ORD record
ord-4b1db29aa7124f76a27a2509c7cb4c3c
Source dataset
uspto-grants-1999_01
Patent number
US05864043

Reaction notes

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