HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecanoyl chloride → 2-phenyl-4-lauroyl-5-phenyl-(3H)-pyrazol-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecanoyl chloride | HCID 8166 | — |
| Reactant | 2-Ethylhexanoyl chloride | HCID 79103 | — |
| Reactant | 1,3-Diphenyl-1H-pyrazol-5-OL | HCID 245736 | — |
| Product | 2-phenyl-4-lauroyl-5-phenyl-(3H)-pyrazol-3-one | HCID 20129861 | — |
Reaction Steps
Followng the procedure of example 18 with the same proportions but replacing 2-phenyl-5-methyl-(3H)-pyrazol-3-one by 2-phenyl-5-phenyl-(3H)-pyrazol-3-one (MW=136.3 g; mp=136° C.) and 2-ethylhexanoyl chloride by lauroyl chloride a solid product is obtained which after recrystallisation in hexane has a melting point of 69° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04761484 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-17bb29af975c41809ad4b7fc4a34ef83 |
| Source note | uspto-grants-1988_08 |