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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 344348Generated: October 29, 2026

Phenyl Isothiocyanate → HCID 54446611, compound

https://huagongshe.com/reaction/344348

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenyl IsothiocyanateHCID 7673—
Reactant4-Amino-5-chloro-2-methoxybenzoic acidHCID 81626—
ReactantHCID 53780052HCID 53780052—
ProductHCID 54446611HCID 54446611—

Reaction Steps

4-(3-tert-Butoxycarbonylaminomethylpyrrolidin-1-yl)butylamine (1.00 g) as starting compound was reacted and treated in the same manner as in Example 34 using phenyl isothiocyanate (0.44 ml) and 4-amino-5-chloro-2-methoxybenzoic acid (0.74 g) to give 4-amino-5-chloro-2-methoxy-N-(1-(4-(3-phenylthioureido)butyl)pyrrolidin-3-ylmethyl)benzamide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05864039
Source datasetuspto-grants-1999_01
ORD IDord-7b56073bccc1477bbe81225d55aa43d1
Source noteuspto-grants-1999_01