HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 53680137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 54352556 | HCID 54352556 | — |
| Product | HCID 53680137 | HCID 53680137 | 52.2% |
Reaction Steps
4-Amino-5-chloro-N-((1-(5-(cyclohexylmethylamino)pentyl)piperidin-4-yl)methyl)-2-methoxybenzamide (0.79 g) as starting compound, benzaldehyde (0.19 g) and sodium cyanoborohydride (0.23 g) were reacted and treated in the same manner as in Example 136 to give 0.49 g of 4-amino-N-((1-(5-(N-benzyl-N-(cyclohexylmethyl)amino)pentyl)piperidin-4-yl)methyl)-5-chloro-2-methoxybenzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05864039 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-47df8ce248574412ba1b8f8047353188 |
| Source note | uspto-grants-1999_01 |