HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54275761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 21887420 | HCID 21887420 | — |
| Reactant | 4-amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochloride | HCID 69966330 | — |
| Product | HCID 54275761 | HCID 54275761 | 10.5% |
Reaction Steps
4-Amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochloride (2.0 g) as starting compound, potassium carbonate (3.0 g) and 6-bromo-1-(2-thienyl)-1-hexanone (1.6 g) were reacted and treated in the same manner as in Example 172 to give 0.27 g of 4-amino-5-chloro-N-((1-(6-oxo-6-(2-thienyl)hexyl)piperidin-4-yl)methyl)-2-methoxybenzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05864039 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-e1ac26db615b4a8195a61c11c535666c |
| Source note | uspto-grants-1999_01 |