HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54063750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 54502525 | HCID 54502525 | — |
| Reactant | 4-amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochloride | HCID 69966330 | — |
| Product | HCID 54063750 | HCID 54063750 | 13.5% |
Reaction Steps
4-Amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochloride (0.96 g) as a starting compound, 6-bromo-1-(3-hydroxyphenyl)-1-hexanone (0.70 g) and potassium carbonate (1.60 g) were reacted and purified in the same manner as in Example 172 to give 0.17 g of 4-amino-5-chloro-2-methoxy-N-((1-(6-(3-hydroxyphenyl)-6-oxohexyl)-piperidin-4-yl)methyl)benzamide as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05864039 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-42a50a53513947af89f77316845da283 |
| Source note | uspto-grants-1999_01 |