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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 344555Generated: October 31, 2026

Potassium Carbonate → HCID 54063750, compound

https://huagongshe.com/reaction/344555

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 54502525HCID 54502525—
Reactant4-amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochlorideHCID 69966330—
ProductHCID 54063750HCID 5406375013.5%

Reaction Steps

4-Amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochloride (0.96 g) as a starting compound, 6-bromo-1-(3-hydroxyphenyl)-1-hexanone (0.70 g) and potassium carbonate (1.60 g) were reacted and purified in the same manner as in Example 172 to give 0.17 g of 4-amino-5-chloro-2-methoxy-N-((1-(6-(3-hydroxyphenyl)-6-oxohexyl)-piperidin-4-yl)methyl)benzamide as a brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05864039
Source datasetuspto-grants-1999_01
ORD IDord-42a50a53513947af89f77316845da283
Source noteuspto-grants-1999_01