HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → N-(7-chloro-2,3-dihydro-2-(hydroxymethyl)-4-benzofuranyl)phthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | 4-Chloro-3-[(prop-2-en-1-yl)oxy]aniline | HCID 54496113 | — |
| Reactant | N-(2-allyl-4-chloro-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide | HCID 57171405 | — |
| Product | N-(7-chloro-2,3-dihydro-2-(hydroxymethyl)-4-benzofuranyl)phthalimide | HCID 15018907 | — |
Reaction Steps
The title compound was prepared, as a white solid, m.p.: 181°-183° C., from 3B and phthalic anhydride in three steps, according to the procedures described for preparing Example 4 from 3D.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05053071 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-62815a2493a34ee78533b0b1f4f0ec87 |
| Source note | uspto-grants-1991_10 |