HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-Methyl-3-(oxazol-2-yl)-pyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(1,3-Oxazol-2-yl)pyridine | HCID 20405387 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Methyl-3-(oxazol-2-yl)-pyridinium iodide | HCID 67925087 | — |
Reaction Steps
11.3 g of [(3-oxazol-2-yl)-pyridine] prepared as indicated in Helv. Chim. Acta 45 375 (1962) and 22.4 g of methyl iodide in 150 cm3 of ethanol are heated under reflux for 2 hours, then the reaction medium is left for 2 days. The solvent is evaporated, the residue is crystallized from 95° ethanol and 17 g of product is obtained. M.p.=241° C. (decomp.) after recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05053416 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-930f310ea1c64ef5ae73e7b18080b2e8 |
| Source note | uspto-grants-1991_10 |