反应详情

温度

120 °C

In an autoclave, 100 ml of water and 3.3 g of calcium carbonate and 10 g of 3-(1-bromoethyl)benzophenone were placed, and were then heated at 120° C. for 6 hours. The resultant reaction solution was extracted with benzene, and a formed benzene layer was then dried with anhydrous sodium sulfate, followed by distilling off the solvent. The resultant product had the spectrum data which were identical with those of 3-(1-hydroxyethyl)benzophenone.

1. customThe resultant reaction solution
2. extractionwas extracted with benzene
3. dry with materiala formed benzene layer was then dried with anhydrous sodium sulfate
4. distillationby distilling off the solvent