HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acenaphthene → Acenaphthylene, dodecahydro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acenaphthene | HCID 6734 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | Acenaphthylene, dodecahydro- | HCID 102215 | 100% |
Reaction Steps
Acenaphthene was hydrogenated by the same procedure as in Example 1 except that the catalyst was replaced by a Raney nickel catalyst. Perhydroacenaphthene was produced in a yield of 100%, but the yields of Nos. 1 to 4 isomers were 18.9%, 8.3%, 37.4%, and 35.4%, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04761510 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-4c6ddff5b3c744a1827fabacb7509121 |
| Source note | uspto-grants-1988_08 |