HCID 54004567, compound → HCID 54205265, compound

Participants

Reaction Steps

A solution was prepared by dissolving 0.2 g of 3,3',5,-5'-tetraallyl-2,4'-biphenyldiol in 10 ml of ethyl acetate. The solution was catalytic reduced with 50 mg of 5% palladium-carbon catalyst at room temperature under normal pressure. The catalyst was filtered out, and the filtrate was concentrated and purified by a silica gel column-chromatography (n-hexane:ethyl acetate=5:1) to yield 0.15 g of 3,3',5,5'-tetrapropyl-2,4'-biphenyldiol.

Provenance & Evidence