Acetic Acid → HCID 53811930, compound

Participants

Reaction Steps

A mixture was prepared by adding 0.2 g of 4-allyl-2-[5-allyl- 2-(6-bromohexyloxy)phenyl]phenol and 0.1 g of silver acetate to 3 ml of acetic acid. The mixture was refluxed by heating for 2 hours and concentrated. The concentrate was extracted with diethylether. The extract was washed with solution sodium hydrogencarbonate and an aqueous solution saturated with NaCl, dried with sodium sulfate and concentrated. The concentrate was purified by a silica gel column-chromatography (n-hexane:ethyl acetate=15:1) to yield 0.12 g of 4-allyl-2-[5allyl-2-(6-acetoxyhexyloxy)phenyl]phenol.

Provenance & Evidence