4-Pentylbenzoyl chloride → 4-(4-Pentylbenzoyloxy)-phenylsulfur pentafluoride

HRID 344979Notes

Reaction equation

HRID 344979 reaction equation
[CH2:1]([C:6]1[CH:14]=[CH:13][C:9]([C:10](Cl)=[O:11])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[OH:15][C:16]1[CH:21]=[CH:20][C:19]([S:22]([F:27])([F:26])([F:25])([F:24])[F:23])=[CH:18][CH:17]=1>N1C=CC=CC=1>[CH2:1]([C:6]1[CH:14]=[CH:13][C:9]([C:10]([O:15][C:16]2[CH:21]=[CH:20][C:19]([S:22]([F:27])([F:23])([F:24])([F:25])[F:26])=[CH:18][CH:17]=2)=[O:11])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 1708124-Pentylbenzoyl chlorideHCID 27792034-Hydroxyphenylsulfur pentafluoride

Product 1

HCID 543285934-(4-Pentylbenzoyloxy)-phenylsulfur pentafluoride

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

A mixture of 11.6 g of p-pentylbenzoyl chloride, 11.1 g of p-hydroxyphenyl sulfur pentafluoride and 100 ml of pyridine is stirred it room temperature for 20 hours. Concentrating the mixture and working it up in the customary manner gives 4-(4-pentylbenzoyloxy)-phenylsulfur pentafluoride.

Workup

  1. concentrationConcentrating the mixture

Sources & evidence

ORD record
ord-16bafe4e88f4466a8b6376367df63408
Source dataset
uspto-grants-1991_10
Patent number
US05055223

Reaction notes

Loading…